Technology Process of C21H23Cl3N4O4S
There total 5 articles about C21H23Cl3N4O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(I) sulfate pentahydrate; sodium L-ascorbate;
In
tetrahydrofuran; water;
at 20 ℃;
for 19h;
DOI:10.5012/bkcs.2011.32.2.664
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C
2: copper(I) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 19 h / 20 °C
With
sodium azide; copper(I) sulfate pentahydrate; sodium L-ascorbate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2011.32.2.664
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 12 h / 150 °C
2: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C
3: copper(I) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 19 h / 20 °C
With
N-Bromosuccinimide; sodium azide; 2,2'-azobis(isobutyronitrile); copper(I) sulfate pentahydrate; sodium L-ascorbate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; benzene;
DOI:10.5012/bkcs.2011.32.2.664