C₁₇H₁₉BrNOP

Base Information

Chemical Name:C₁₇H₁₉BrNOP
CAS No.:1616558-16-7
Molecular Formula:C₁₇H₁₉BrNOP
Molecular Weight:364.222
Hs Code.:

Synonyms:C₁₇H₁₉BrNOP

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Chemical Property of C₁₇H₁₉BrNOP

Chemical Property:

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Technology Process of C₁₇H₁₉BrNOP

There total 5 articles about C₁₇H₁₉BrNOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1616557-91-5
C₁₀H₁₀BrOP

: 100-46-9
benzylamine

: 1616558-16-7
C₁₇H₁₉BrNOP

Guidance literature:: In water; at 90 ℃;
DOI:10.1016/j.bmcl.2014.05.036

Reference yield:

: 20677-12-7
diethyl (4-bromophenyl)phosphonate

: 1616558-16-7
C₁₇H₁₉BrNOP

Guidance literature:: Multi-step reaction with 4 steps

1: trimethylsilyl bromide

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane

3: tetrahydrofuran / -78 °C

4: water / 90 °C

With oxalyl dichloride; trimethylsilyl bromide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2014.05.036

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 1616558-16-7
C₁₇H₁₉BrNOP

Guidance literature:: Multi-step reaction with 5 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine; potassium acetate / tetrahydrofuran / 22 h / 68 °C

2: trimethylsilyl bromide

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane

4: tetrahydrofuran / -78 °C

5: water / 90 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; oxalyl dichloride; trimethylsilyl bromide; potassium acetate; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2014.05.036