1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione

Base Information

• Chemical Name: 1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione
• CAS No.: 1433416-27-3
• Molecular Formula: C₂₃H₂₄FeO₃
• Molecular Weight: 404.289
• Mol file: 1433416-27-3.mol

Synonyms:1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione

Chemical Property of 1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione

There total 1 articles about 1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1-ferrocenylethanol (1277-49-2) + 1-(4-methoxyphenyl)butan-1,3-dione (4023-80-7) → 1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione (1433416-27-3)

Guidance literature:

1-ferrocenylethanol; 1-(4-methoxyphenyl)butan-1,3-dione; In acetonitrile; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

With ammonium cerium (IV) nitrate; In acetonitrile; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2013.03.032

Reference yield: 50.0%

1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione (1433416-27-3) → 1-(4-methoxyphenyl)-3-ferrocenylbutane-1-one

Guidance literature:

1-(4-methoxyphenyl)-2-(1-ferrocenylethyl)-butane-1,3-dione; With acetic acid; In toluene; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

With ethylenediamine; In toluene; for 12h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1016/j.jorganchem.2014.07.019

upstream raw materials:

1-ferrocenylethanol

1-(4-methoxyphenyl)butan-1,3-dione