(Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate

Base Information

Chemical Name:(Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate
CAS No.:1213766-92-7
Molecular Formula:C₂₃H₂₁NO₄
Molecular Weight:375.424
Hs Code.:

Synonyms:(Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate

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Chemical Property of (Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate

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Technology Process of (Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate

There total 2 articles about (Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1213766-86-9
(E)-benzyl 3-[1-(2-iodo-4,5-dimethoxybenzyl)-1H-pyrrol-2-yl]acrylate

: 1213766-92-7
(Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate

: 1213766-91-6
(E)-benzyl 3-(7,8-dimethoxy-5H-pyrrolo[2,1-a]isoindol-3-yl)acrylate

Guidance literature:: With tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate; triphenylphosphine; In acetonitrile; at 60 ℃; for 8h; Inert atmosphere;
DOI:10.1002/adsc.200900368

Reference yield: 42.0%

: 1213766-86-9
(E)-benzyl 3-[1-(2-iodo-4,5-dimethoxybenzyl)-1H-pyrrol-2-yl]acrylate

: 1213766-92-7
(Z)-benzyl 2-(7,8-dimethoxypyrrolo[1,2-b]isoquinolin-10-ylidene)acetate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; In acetonitrile; for 16h; Inert atmosphere; Reflux;
DOI:10.1002/adsc.200900368