4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

Base Information

Chemical Name:4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate
CAS No.:41623-84-1
Molecular Formula:C₂₄H₃₀O₁₃
Molecular Weight:526.494
Hs Code.:

Synonyms:4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

Chemical Property:

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Technology Process of 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

There total 2 articles about 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose

: 57404-55-4
4-acetoxymethyl-2-methoxyphenol

: 41623-84-1
4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 498-00-0
4-hydroxymethyl-2-methoxyphenol

: 41623-84-1
4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: Novozym 435 / 69 h / 65 °C / Enzymatic reaction

2: triphenylphosphine; diethylazodicarboxylate / toluene / 3 h / 20 °C / Inert atmosphere

With Novozym 435; triphenylphosphine; diethylazodicarboxylate; In toluene;

Reference yield: 74.0%

: 41623-84-1
4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate

: 4-(β-D-glucopyranosyloxy)-3-methoxybenzyl alcohol

Guidance literature:: 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-3-methoxybenzyl acetate; With methanol; sodium methylate; at 20 ℃; for 3h;