N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

Base Information

Chemical Name:N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide
CAS No.:864949-55-3
Molecular Formula:C₂₆H₃₃NO₄S₂Si
Molecular Weight:515.77
Hs Code.:

Synonyms:N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

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Chemical Property of N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

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Technology Process of N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

There total 5 articles about N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(3-benzenesulfinyl-5-methyl-hexa-3,4-dienyl)-4-methyl-N-(3-trimethylsilanyl-prop-2-ynyl)-benzenesulfonamide

: 864949-55-3
N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1021/jo050770z

Reference yield:

: 864949-48-4
N-(5-hydroxy-5-methyl-3-hexynyl)-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

: 864949-55-3
N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / -78 °C

2: m-CPBA / CH₂Cl₂ / 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo050770z

Reference yield:

: 4-methyl-N-[5-methyl-5-(tetrahydro-pyran-2-yloxy)-hex-3-ynyl]-N-(3-trimethylsilanyl-prop-2-ynyl)-benzenesulfonamide

: 864949-55-3
N-[5-methyl-3-(phenylsulfonyl)-3,4-hexadienyl]-N-[3-(trimethylsilyl)-2-propynyl]-(4-methylbenzene)sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: PPTS / ethanol / 55 °C

2: Et₃N / tetrahydrofuran / -78 °C

3: m-CPBA / CH₂Cl₂ / 0 °C

With pyridinium p-toluenesulfonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo050770z