4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

Base Information

Chemical Name:4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester
CAS No.:872522-09-3
Molecular Formula:C₂₈H₃₅NO₇
Molecular Weight:497.588
Hs Code.:

Synonyms:4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

Suppliers and Price of 4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

There total 1 articles about 4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 872522-07-1
4-(S)-hydroxy-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 872522-09-3
4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: With lanthanum(lll) triflate; In toluene; at 20 ℃; for 4h;
DOI:10.1016/j.bioorg.2005.08.001

Reference yield: 29.0%

: 872522-09-3
4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

: 872522-11-7
(2S,4S)-4-(4-methoxy-benzyloxy)-6-oxo-piperidine-2-carboxylic acid benzyl ester

Guidance literature:: 4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester; With iodine; In tetrahydrofuran; water; for 0.5h;

In benzene; for 4h; Further stages.; Heating;
DOI:10.1016/j.bioorg.2005.08.001

Reference yield:

: 872522-09-3
4-(S)-(4-methoxy-benzyloxy)-2-(S)-(pent-4-enoyl)amino-hexanedioic acid 1-benzyl ester 6-ethyl ester

: 653589-27-6
(2S,4S)-4-hydroxy-6-oxo-piperidine-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / tetrahydrofuran; H₂O / 0.5 h

1.2: 29 percent / benzene / 4 h / Heating

2.1: 99 percent / TFA / 0.33 h / 20 °C

With iodine; trifluoroacetic acid; In tetrahydrofuran; water;
DOI:10.1016/j.bioorg.2005.08.001