tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Base Information

• Chemical Name: tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)
• CAS No.: 97878-02-9
• Molecular Formula: C₁₆H₃₆N*C₂₄H₈F₁₇O₂Si
• Molecular Weight: 921.853

Synonyms:tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Chemical Property of tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

There total 6 articles about tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(TB-5-11)-bis-(1,1,1,3,3,3-hexafluoro-2-phenyl-propan-2-olato(2-)-C2',O)-phenyl-silicate(1-); lithium salt (70083-67-9) → tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>(pentafluorophenyl)silicate(1-) (97878-02-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 59.6 percent / CH₂Cl₂

2: 72 percent / Br₂ / 24 h / 25 °C

3: 1.) THF; 2.) ether, -78 deg C, then RT, 1 h

With bromine; In dichloromethane;

DOI:10.1021/ja00308a030

Reference yield:

Tetramethylammonium Bis<α,α-bis(trifluoromethyl)-benzenemethanolato(2-)-C2,O>phenylsilicate (70083-69-1) → tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>(pentafluorophenyl)silicate(1-) (97878-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / Br₂ / 24 h / 25 °C

2: 1.) THF; 2.) ether, -78 deg C, then RT, 1 h

With bromine;

DOI:10.1021/ja00308a030

Reference yield:

tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>phenylsilicate(1-) (97878-00-7) → tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>(pentafluorophenyl)silicate(1-) (97878-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / Br₂ / 24 h / 25 °C

2: 1.) THF; 2.) ether, -78 deg C, then RT, 1 h

With bromine;

DOI:10.1021/ja00308a030

upstream raw materials:

(TB-5-11)-bis-(1,1,1,3,3,3-hexafluoro-2-phenyl-propan-2-olato^(2-)-C^2',O)-phenyl-silicate^(1-); lithium salt

Tetramethylammonium Bis<α,α-bis(trifluoromethyl)-benzenemethanolato(2-)-C²,O>phenylsilicate

tetraethylammonium bis<α,α-bis(trifluorometyl)benzenemethanolato(2-)-C²,O>-n-butylsilicate(1-)

tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>phenylsilicate(1-)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 97878-02-9 tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Send

Send

Metric Ton KG G Pound L ML

Send

Send