α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane

Base Information

Chemical Name:α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane
CAS No.:180684-36-0
Molecular Formula:C₂₅H₃₄N₈O₅
Molecular Weight:526.596
Hs Code.:

α-N-(t-butoxycarbonyl)-N<sup>g</sup>-nitro-argininal-semicarbazonyl-4-N-diphenylmethane

Synonyms:α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane

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Technology Process of α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane

There total 4 articles about α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: semicarbazidyl-4-diphenylmethane trifluoroacetate salt

: 186261-75-6
Boc-Arg(NO₂)-H

: 180684-36-0
C₂₅H₃₄N₈O₅

Guidance literature:: With sodium acetate; In ethanol; water; Heating;
DOI:10.1016/S0960-894X(97)00005-X

Reference yield: 78.0%

: 71413-14-4
alpha-N-(t-butoxycarbonyl)-N^g-nitroargininal

: semicarbazidyl-4-diphenylmethane trifluoroacetate salt

: 180684-36-0
α-N-(t-butoxycarbonyl)-N^g-nitro-argininal-semicarbazonyl-4-N-diphenylmethane

Guidance literature:: With sodium acetate; In ethanol; water; for 1h; Heating;
DOI:10.1016/S0040-4039(00)76776-1

Reference yield:

: 2188-18-3
N^α-t-butoxycarbonyl-N^ω-nitro-L-arginine

: 180684-36-0
C₂₅H₃₄N₈O₅

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) i-BuOCOCl, NMP, 2.) MeONHMe, 3.) LiAlH₄, 4.) KHSO₄

2: 90 percent / NaOAc / ethanol; H₂O / Heating

With 1-methyl-pyrrolidin-2-one; potassium hydrogensulfate; lithium aluminium tetrahydride; sodium acetate; N,0-dimethylhydroxylamine; isobutyl chloroformate; In ethanol; water;
DOI:10.1016/S0960-894X(97)00005-X