[2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

Base Information

Chemical Name:[2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol
CAS No.:207272-65-9
Molecular Formula:C₂₁H₂₀O₇
Molecular Weight:384.386
Hs Code.:

Synonyms:[2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

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Technology Process of [2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

There total 14 articles about [2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 207272-63-7
2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-furan-3,4-dicarboxylic acid diethyl ester

: 207272-65-9
[2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 8h; Heating;
DOI:10.1039/a700131b

Reference yield: 84.0%

: C₂₃H₂₀O₉

: 207272-65-9
[2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 23 ℃;
DOI:10.1039/c9sc02682g

Reference yield:

: 81581-26-2
3,4-Methylendioxybenzoyl-acetessigsaeure-ethylester

: 207272-65-9
[2-Benzo[1,3]dioxol-5-yl-5-(3,4-dimethoxy-phenyl)-4-hydroxymethyl-furan-3-yl]-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: NH₃, NH₄Cl

2: Br₂

3: 1.) NaH / 1.) CH₂Cl₂, reflux, 15 min, 2.) CH₂Cl₂, reflux, 3 h

4: 79 percent / TsOH / benzene / 8 h / Heating

5: 95 percent / LiAlH₄ / tetrahydrofuran / 8 h / Heating

With lithium aluminium tetrahydride; ammonia; bromine; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1039/a700131b