<(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

Base Information

Chemical Name:<(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester
CAS No.:161083-47-2
Molecular Formula:C₂₆H₃₄N₄O₆
Molecular Weight:498.579
Hs Code.:

<(2R)-2-<N-(methoxycarbonyl)amino>-2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

Synonyms:<(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

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Chemical Property of <(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

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Technology Process of <(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

There total 3 articles about <(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 161083-57-4
<(2R)-3--2--2-methylpropanoyl>-phenylalanyl-phenylalanine methyl ester

: 161083-47-2
<(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 14h;
DOI:10.1002/hlca.19940770728

Reference yield:

: 161083-41-6
(2R)-3--2--2-methylpropanoic acid

: 161083-47-2
<(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylethylamine / CH₂Cl₂ / 2 h / -18 °C

2: diisopropylethylamine / CH₂Cl₂ / 1.) -18 deg C, 2 h; 2.) r.t., 12 h

3: 99 percent / H₂ / 10percent Pd/C / ethanol / 14 h

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1002/hlca.19940770728

Reference yield:

: C₂₁H₂₇N₄O₁₁P

: 161083-47-2
<(2R)-2--2-methyl-3-(methylamino)propanoyl>-phenylalanyl-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylethylamine / CH₂Cl₂ / 1.) -18 deg C, 2 h; 2.) r.t., 12 h

2: 99 percent / H₂ / 10percent Pd/C / ethanol / 14 h

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1002/hlca.19940770728