Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester
CAS No.:191216-63-4
Molecular Formula:C₅₃H₅₉NO₁₃S
Molecular Weight:950.116
Hs Code.:

Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Synonyms:Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

There total 2 articles about Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 69892-44-0
methyl 2-acetylamino-3-O-benzyl-2-deoxy-α-D-glucopyranoside

: 191216-55-4
Succinic acid mono-((2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl) ester

: 191216-63-4
Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Guidance literature:: With dmap; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In pyridine; at 100 ℃; for 12h;
DOI:10.1016/S0040-4039(97)00729-6

Reference yield:

: 127299-77-8,130781-28-1,138181-68-7,130781-27-0
Phenyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 191216-63-4
Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / DMAP / pyridine / 48 h / Heating

2: 65 percent / DMAP, TosOH, DCC / pyridine / 12 h / 100 °C

With dmap; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In pyridine;
DOI:10.1016/S0040-4039(97)00729-6

Reference yield: 29.0%

: 191216-63-4
Succinic acid (2R,3S,4R,5R,6S)-5-acetylamino-4-benzyloxy-3-hydroxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester (2S,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

: N-((2R,3R,4S,4aR,11aR,13S,14R,15R,15aS,16aS)-3,4,15-Tris-benzyloxy-2-benzyloxymethyl-13-methoxy-6,9-dioxo-tetradecahydro-1,5,10,12,16-pentaoxa-dibenzo[a,d]cyclododecen-14-yl)-acetamide

: N-((2R,3R,4S,4aR,11aR,13S,14R,15R,15aS,16aR)-3,4,15-Tris-benzyloxy-2-benzyloxymethyl-13-methoxy-6,9-dioxo-tetradecahydro-1,5,10,12,16-pentaoxa-dibenzo[a,d]cyclododecen-14-yl)-acetamide

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at -40 ℃; for 0.5h;
DOI:10.1016/S0040-4039(97)00729-6