C₁₉H₂₀N₂O

Base Information

• Chemical Name: C₁₉H₂₀N₂O
• CAS No.: 1421276-34-7
• Molecular Formula: C₁₉H₂₀N₂O
• Molecular Weight: 292.381
• Mol file: 1421276-34-7.mol

Synonyms:C₁₉H₂₀N₂O

Chemical Property of C₁₉H₂₀N₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₀N₂O

There total 2 articles about C₁₉H₂₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

Azobenzene (1227476-15-4) + cyclohexanecarbaldehyde (2043-61-0) → C19H20N2O (1421276-34-7)

Guidance literature:

With tert.-butylhydroperoxide; palladium diacetate; In 1,2-dichloro-ethane; at 80 ℃; for 12h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/ol303434n

Reference yield:

aniline (62-53-3) → C19H20N2O (1421276-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(I) bromide

2: palladium diacetate; tert.-butylhydroperoxide / 1,2-dichloro-ethane / 12 h / 80 °C / Inert atmosphere; Sealed tube

With tert.-butylhydroperoxide; palladium diacetate; copper(I) bromide; In 1,2-dichloro-ethane;

DOI:10.1021/ol303434n

Reference yield: 99.0%

C19H20N2O (1421276-34-7) → 2-phenyl-3-cyclohexanyl-2H-indazole (1421276-52-9)

Guidance literature:

With toluene-4-sulfonic acid hydrazide; In ethanol; at 110 ℃; for 1h;

DOI:10.1002/adsc.201801055

upstream raw materials:

Azobenzene

cyclohexanecarbaldehyde

aniline

Downstream raw materials:

2-phenyl-3-cyclohexanyl-2H-indazole