Technology Process of C38H46O5Si
There total 8 articles about C38H46O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; N-butylamine;
palladium on activated charcoal;
In
methanol;
at 20 ℃;
for 2h;
DOI:10.1016/j.tetlet.2007.07.176
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 80 percent / NaH; TBAI / tetrahydrofuran / 12 h / 0 °C
2.1: NMO; OsO4 / acetone; H2O / 24 h / 20 °C
2.2: NaIO4 / tetrahydrofuran; H2O / 1 h / 0 °C
2.3: 70 percent / CH2Cl2 / 6 h / 20 °C
3.1: 90 percent / H2; n-BuNH2 / Pd/C / methanol / 2 h / 20 °C
With
osmium(VIII) oxide; N-methyl-2-indolinone; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; N-butylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; water; acetone;
2.3: Wittig olefination reaction;
DOI:10.1016/j.tetlet.2007.07.176
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: NMO; OsO4 / acetone; H2O / 24 h / 20 °C
1.2: NaIO4 / tetrahydrofuran; H2O / 1 h / 0 °C
1.3: 70 percent / CH2Cl2 / 6 h / 20 °C
2.1: 90 percent / H2; n-BuNH2 / Pd/C / methanol / 2 h / 20 °C
With
osmium(VIII) oxide; N-methyl-2-indolinone; hydrogen; N-butylamine;
palladium on activated charcoal;
In
methanol; water; acetone;
1.3: Wittig olefination reaction;
DOI:10.1016/j.tetlet.2007.07.176