O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate
CAS No.:1400594-79-7
Molecular Formula:C₄₁H₃₅Cl₃N₄O₇
Molecular Weight:802.111
Hs Code.:

Synonyms:O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate

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Chemical Property of O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate

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Technology Process of O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate

There total 1 articles about O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₃₉H₃₅N₃O₇

: 545-06-2
trichloroacetonitrile

: 1400594-79-7
O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With sodium hydride; In dichloromethane; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja3069962

Reference yield: 54.0%

: 1400594-79-7
O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)]-α-D-glucopyranosyl trichloroacetimidate

: 1400595-06-3
dimethylthexylsilyl O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: 1400595-02-9
dimethylthexylsilyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: C₈₈H₉₈Cl₃N₇O₁₉Si

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; at -55 - 0 ℃; for 1.5h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja3069962