(2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

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Chemical Name:(2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester
CAS No.:1009093-08-6
Molecular Formula:C₂₀H₃₃NO₃Si
Molecular Weight:363.572
Hs Code.:

Synonyms:(2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

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Chemical Property of (2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

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Technology Process of (2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

There total 9 articles about (2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1009093-07-5
C₂₁H₃₇NO₆SSi

: 1009093-08-6
(2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 1009094-58-9
C₁₅H₂₄N₂O₅S

: 1009093-08-6
(2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dmap / dichloromethane / 3.5 h / 0 - 20 °C

2: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C

With potassium tert-butylate; triethylamine; dmap; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1009094-17-0
C₂₀H₃₆N₂O₃Si

: 1009093-08-6
(2S,3S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-phenyl-aziridine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3: triethylamine / dmap / dichloromethane / 3.5 h / 0 - 20 °C

4: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C

With potassium tert-butylate; tetrabutyl ammonium fluoride; triethylamine; dmap; In tetrahydrofuran; dichloromethane;