2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

Base Information

Chemical Name:2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline
CAS No.:1126425-86-2
Molecular Formula:C₁₉H₂₉ClN₂Si
Molecular Weight:348.991
Hs Code.:

Synonyms:2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

There total 4 articles about 2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 59772-49-5
2-bromo-6-chloroaniline

: 365564-11-0
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

: 1126425-86-2
2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In water; butan-1-ol; at 35 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol8026957

Reference yield: 81.0%

: 13420-63-8
2-chloro-6-iodobenzoic acid

: 365564-11-0
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

: 1126425-86-2
2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

: C₁₉H₂₉ClN⁽¹⁵⁾NSi

Guidance literature:: 2-chloro-6-iodobenzoic acid; With sulfuric acid; at 60 ℃; for 1h; Inert atmosphere;

With [⁽¹⁵⁾N]sodium azide; at 20 ℃; for 42h; Inert atmosphere;

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole; With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In water; butan-1-ol; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00098

Reference yield: 75.0%

: 84483-28-3
2-chloro-6-iodoaniline

: 365564-11-0
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

: 1126425-86-2
2-chloro-6-(1-(triisopropylsilyl)-1H-pyrrol-3-yl)aniline

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In water; butan-1-ol; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00098