C₁₆H₁₄F₂O₃S

Base Information

Chemical Name:C₁₆H₁₄F₂O₃S
CAS No.:1246013-27-3
Molecular Formula:C₁₆H₁₄F₂O₃S
Molecular Weight:324.348
Hs Code.:

C<sub>16</sub>H<sub>14</sub>F<sub>2</sub>O<sub>3</sub>S

Synonyms:C₁₆H₁₄F₂O₃S

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Chemical Property of C₁₆H₁₄F₂O₃S

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Technology Process of C₁₆H₁₄F₂O₃S

There total 4 articles about C₁₆H₁₄F₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 949102-16-3
C₉H₇F₃O₂S

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 1246013-27-3
C₁₆H₁₄F₂O₃S

Guidance literature:: 2-methoxyphenylmagnesium bromide; With copper(l) cyanide; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

C₉H₇F₃O₂S; In tetrahydrofuran; at -78 ℃; for 1h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/asia.201000022

Reference yield:

: 1246013-18-2
4-methylphenyl-1,2,2-trifluorovinyl sulfide

: 1246013-27-3
C₁₆H₁₄F₂O₃S

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / Reflux

2.1: copper(l) cyanide / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

With copper(l) cyanide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/asia.201000022

Reference yield:

: 10486-08-5
sodium p-thiocresolate

: 1246013-27-3
C₁₆H₁₄F₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N-dimethyl-formamide / 3 h / -60 °C

2.1: ethylmagnesium bromide / tetrahydrofuran / 3 h / 0 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / Reflux

4.1: copper(l) cyanide / tetrahydrofuran / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

With ethylmagnesium bromide; copper(l) cyanide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000022