(2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine

Base Information

Chemical Name:(2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine
CAS No.:1258505-20-2
Molecular Formula:C₂₄H₃₁NO₁₀
Molecular Weight:493.511
Hs Code.:

Synonyms:(2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine

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Chemical Property of (2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine

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Technology Process of (2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine

There total 1 articles about (2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1258505-13-3
3,4-di-O-acetyl-1,4-anhydro-N-(2,2-diethoxycarbonylvinyl)-α-L-arabinopyranosylamine

: 100-51-6,185532-71-2
benzyl alcohol

: 1258505-28-0
(2R,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine

: 1258505-20-2
(2S,3R,4S,5S)-3,4-di-acetoxy-2-benzyloxy-N-(2,2-diethoxycarbonylvinyl)-5-hydroxymethylpyrrolidine

Guidance literature:: 3,4-di-O-acetyl-1,4-anhydro-N-(2,2-diethoxycarbonylvinyl)-α-L-arabinopyranosylamine; With boron trifluoride diethyl etherate; In diethyl ether; at 0 ℃; Molecular sieve; Inert atmosphere;

benzyl alcohol; In diethyl ether; at 20 ℃; for 1h; optical yield given as %de; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.09.065