10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

Base Information

Chemical Name:10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene
CAS No.:1319194-03-0
Molecular Formula:C₂₉H₃₁OPS
Molecular Weight:458.604
Hs Code.:

Synonyms:10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

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Chemical Property of 10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

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Technology Process of 10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

There total 4 articles about 10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1319194-01-8
10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

: 1319194-03-0
10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

Guidance literature:: With dihydrogen peroxide; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ic201116p

Reference yield:

: 1263143-03-8
3-bromo-2-(2-bromophenyl)benzo[b]thiophene

: 1319194-03-0
10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / 2 h / -78 - 20 °C / Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: dihydrogen peroxide / dichloromethane / 16 h / 20 °C / Inert atmosphere

With n-butyllithium; dihydrogen peroxide; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ic201116p

Reference yield:

: 6287-82-7
2,3-dibromobenzo[b]thiophene

: 1319194-03-0
10-oxo-10-(2,4,6-triisopropylphenyl)-10H-benzo[b]phosphindolo[2,3-d]thiophene

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / 16 h / 100 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 2 h / -78 - 20 °C / Inert atmosphere

2.2: 16 h / 20 °C / Inert atmosphere

3.1: dihydrogen peroxide / dichloromethane / 16 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dihydrogen peroxide; sodium carbonate; In 1,4-dioxane; diethyl ether; hexane; dichloromethane; water; 1.1: Suzuki coupling;
DOI:10.1021/ic201116p