2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide

Base Information

Chemical Name:2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide
CAS No.:6556-77-0
Molecular Formula:C15H11ClN2OS
Molecular Weight:334.412
Hs Code.:
DSSTox Substance ID:DTXSID60368153
Wikidata:Q82154507

Synonyms:6556-77-0;Enamine_001762;Oprea1_867975;2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide;DTXSID60368153;HMS1399A02;AKOS000859390;Z18459715

Suppliers and Price of 2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide

Chemical Property:

Vapor Pressure:2.5E-10mmHg at 25°C
Boiling Point:505.1°C at 760 mmHg
Flash Point:259.3°C
Density:1.36g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:302.0280618
Heavy Atom Count:20
Complexity:381

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)SCC(=O)NC2=CC=CC(=C2)C#N)Cl

Technology Process of 2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide

There total 4 articles about 2-(2-chlorophenyl)sulfanyl-N-(3-cyanophenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4341-76-8
Ethyl 2-butynoate

: 42370-85-4
4,4-(ethylenedioxy)-1-ethynyl-2,6,6-trimethylcyclohex-2-en-1-ol

: 6556-77-0
ethyl (Z)-5-[4',4'-(ethylenedioxy)-1'-hydroxy-2',6',6'-trimethylcyclohex-2'-enyl]-3-methylpent-2-en-4-ynoate

Guidance literature:: With palladium diacetate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 20h;

Reference yield:

: 14203-64-6
7,9,9-trimethyl-1,4-dioxa-spiro[4.5]dec-6-en-8-one

: 6556-77-0
ethyl (Z)-5-[4',4'-(ethylenedioxy)-1'-hydroxy-2',6',6'-trimethylcyclohex-2'-enyl]-3-methylpent-2-en-4-ynoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / hexane; tetrahydrofuran / 0.25 h / -78 °C

1.2: 90 percent / hexane; tetrahydrofuran / 1 h / -78 - 20 °C

2.1: 91 percent / K₂CO₃ / methanol / 2 h / 20 °C

3.1: 5.7 g / palladium(II) acetate; triphenylphosphine / tetrahydrofuran / 20 h / 20 °C

With palladium diacetate; potassium carbonate; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane;

Reference yield:

: 663601-46-5
4,4-(ethylenedioxy)-2,6,6-trimethyl-1-trimethylsilanylethynylcyclohex-2-en-1-ol

: 6556-77-0
ethyl (Z)-5-[4',4'-(ethylenedioxy)-1'-hydroxy-2',6',6'-trimethylcyclohex-2'-enyl]-3-methylpent-2-en-4-ynoate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / K₂CO₃ / methanol / 2 h / 20 °C

2: 5.7 g / palladium(II) acetate; triphenylphosphine / tetrahydrofuran / 20 h / 20 °C

With palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol;