(endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane>

Base Information

• Chemical Name: (endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane>
• CAS No.: 86146-95-4
• Molecular Formula: C₁₆H₁₉ClS
• Molecular Weight: 278.846

Synonyms:(endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane>

Chemical Property of (endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane>

Chemical Property:

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Technology Process of (endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane>

There total 2 articles about (endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

p-methylbenzenesulfenyl chloride (933-00-6) + spirohept-5-ene-2,1'-cyclopropane> (6572-50-5) → (exo-2)-6-chloro-2-(p-tolylthio)tricyclo<4.2.1.03,7>nonane (86146-93-2) + (endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane> (86146-95-4) + (1R,3aR,5R,6R,6aR)-1-Chloro-6-p-tolylsulfanyl-octahydro-1,5-methano-pentalene (86146-94-3)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/ja00353a046

Reference yield: 10.0%

p-methylbenzenesulfenyl chloride (933-00-6) + 5-spirocyclopropylnorbornene (6572-50-5) → (exo-2)-6-chloro-2-(p-tolylthio)tricyclo<4.2.1.03,7>nonane (86146-93-2) + (endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane> (86146-95-4) + (anti-8)-3-chloro-8-(p-tolylthio)tricyclo<4.2.1.03,7>nonane (86146-94-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.5h;

Reference yield: 89.0%

(endo-5,exo-6)-5-chloro-6-(p-tolylthio)spiroheptane-2,1'-cyclopropane> (86146-95-4) → (endo-5,exo-6)-5-chloro-6-(p-tolylsulfonyl)spiroheptane-2,1'-cyclopropane> (106435-04-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 48h;

upstream raw materials:

p-methylbenzenesulfenyl chloride

5-spirocyclopropylnorbornene

spirohept-5-ene-2,1'-cyclopropane>

Downstream raw materials:

(endo-5,exo-6)-5-chloro-6-(p-tolylsulfonyl)spiroheptane-2,1'-cyclopropane>

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