dibenzo[d,f][1,3]dioxepin

Base Information

Chemical Name:dibenzo[d,f][1,3]dioxepin
CAS No.:220-11-1
Molecular Formula:C₁₃H₁₀O₂
Molecular Weight:198.221
Hs Code.:

Synonyms:dibenzo[d,f][1,3]dioxepin

Suppliers and Price of dibenzo[d,f][1,3]dioxepin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of dibenzo[d,f][1,3]dioxepin

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of dibenzo[d,f][1,3]dioxepin

There total 4 articles about dibenzo[d,f][1,3]dioxepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1443418-23-2
C₁₃H₁₁BrO₂

: 220-11-1
dibenzo[d,f][1,3]dioxepin

: 90-43-7,287950-96-3
2-Phenylphenol

Guidance literature:: With pyridine; potassium tert-butylate; (R)-1,1'-binaphthyl-2,2'-diamine; at 120 ℃; for 2h; Solvent; Reagent/catalyst; Time; Temperature; Inert atmosphere; Microwave irradiation;
DOI:10.1002/chem.201301969

Reference yield:

: 95-56-7
2-hydroxybromobenzene

: 220-11-1
dibenzo[d,f][1,3]dioxepin

: 90-43-7,287950-96-3
2-Phenylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide

2: sulfuryl dichloride / dichloromethane

3: potassium carbonate / N,N-dimethyl-formamide

4: potassium tert-butylate; (R)-1,1'-binaphthyl-2,2'-diamine / pyridine / 2 h / 120 °C / Microwave irradiation; Inert atmosphere

With sulfuryl dichloride; potassium tert-butylate; sodium hydride; potassium carbonate; (R)-1,1'-binaphthyl-2,2'-diamine; In pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201207485

Reference yield:

: 592508-12-8
1-bromo-2-[(methylsulfanyl)methoxy]benzene

: 220-11-1
dibenzo[d,f][1,3]dioxepin

: 90-43-7,287950-96-3
2-Phenylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuryl dichloride / dichloromethane

2: potassium carbonate / N,N-dimethyl-formamide

3: potassium tert-butylate; (R)-1,1'-binaphthyl-2,2'-diamine / pyridine / 2 h / 120 °C / Microwave irradiation; Inert atmosphere

With sulfuryl dichloride; potassium tert-butylate; potassium carbonate; (R)-1,1'-binaphthyl-2,2'-diamine; In pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201207485