IMidafenacin IMpurity (1-(3-Cyano-3,3-Diphenylpropyl)-2-Methyl-1H-IMidazoliuM Phosphate)

Base Information

Chemical Name:IMidafenacin IMpurity (1-(3-Cyano-3,3-Diphenylpropyl)-2-Methyl-1H-IMidazoliuM Phosphate)
CAS No.:562091-56-9
Molecular Formula:C₂₀H₁₉N₃*H₃O₄P
Molecular Weight:399.386
Hs Code.:
Mol file:562091-56-9.mol

Synonyms:4-(2-methyl-1-imidazolyl)-2,2-diphenylbutyronitrile phosphate

Suppliers and Price of IMidafenacin IMpurity (1-(3-Cyano-3,3-Diphenylpropyl)-2-Methyl-1H-IMidazoliuM Phosphate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 7 raw suppliers

Chemical Property of IMidafenacin IMpurity (1-(3-Cyano-3,3-Diphenylpropyl)-2-Methyl-1H-IMidazoliuM Phosphate)

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of IMidafenacin IMpurity (1-(3-Cyano-3,3-Diphenylpropyl)-2-Methyl-1H-IMidazoliuM Phosphate)

There total 4 articles about IMidafenacin IMpurity (1-(3-Cyano-3,3-Diphenylpropyl)-2-Methyl-1H-IMidazoliuM Phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 214777-43-2
4-(2-methyl-1H-imidazol-1-yl)-2,2-diphenylbutanenitrile

: 562091-56-9
4-(2-methyl-1-imidazolyl)-2,2-diphenylbutyronitrile phosphate

Guidance literature:: With phosphoric acid; In ethanol; water; at 30 - 31 ℃; for 16.5h;

Reference yield: 68.0%

: 562091-56-9
4-(2-methyl-1-imidazolyl)-2,2-diphenylbutyronitrile phosphate

Guidance literature:: In water; isopropyl alcohol; at 15 ℃; for 1h; Purification / work up;

Reference yield:

: 39186-58-8
4-bromo-2,2-diphenylbutyronitrile

: 562091-56-9
4-(2-methyl-1-imidazolyl)-2,2-diphenylbutyronitrile phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol; water / 5 h / 40 °C

2: thionyl chloride; pyridine / tetrahydrofuran / 5 h / 50 °C

With pyridine; thionyl chloride; sodium hydroxide; In tetrahydrofuran; methanol; water;