4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside

Base Information

Chemical Name:4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside
CAS No.:112146-42-6
Molecular Formula:C₂₉H₃₃NO₁₂
Molecular Weight:587.581
Hs Code.:

Synonyms:4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside

Suppliers and Price of 4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside

Chemical Property:

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Technology Process of 4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside

There total 31 articles about 4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 111275-60-6,111322-26-0,131177-33-8,131177-34-9
4'-O-benzyloxycarbonyl-4-O-(2-benzyloxycarbonylamino-2-deoxy-4,6-O-ethylidene-α-D-glucopyranosyl)-4'-O-demethyl-4-epipodophyllotoxin

: 105656-01-7,111322-27-1,112146-42-6,112246-51-2,112317-52-9,112318-79-3,134623-83-9
4-O-(2-amino-2-deoxy-4,6-O-ethylidene-α-D-glucopyranosyl)-4'-O-demethyl-4-epipodophyllotoxin

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; under 735.5 Torr;
DOI:10.1016/0008-6215(90)80062-8

Reference yield: 75.0%

: 111275-60-6,111322-26-0,131177-33-8,131177-34-9
1-O-(2-benzyloxycarbonylamino-2-deoxy-4:6-O-ethylidene-β-D-glucopyranosyl)-4'-O-benzyloxycarbonyl-4'-O-demethyl-1-epipodophyllotoxin

: 105656-01-7,111322-27-1,112146-42-6,112246-51-2,112317-52-9,112318-79-3,134623-83-9
1-O-(2-amino-2-deoxy-4:6-O-ethylidene-β-D-glucopyranosyl)-4'-O-demethyl-1-epipodophyllotoxin

Guidance literature:: With hydrogen; palladium; In methanol; ethyl acetate; for 8h;
DOI:10.1248/cpb.34.3733

Reference yield:

: C₄₅H₄₂N₆O₁₅

: 112146-42-6
4′-demethyl-(epi)-podophyllotoxin 4-O-2″-deoxy-2″-amino-4″,6″-di-O-ethylidene-β-D-glucopyranoside

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol; at -78 - 20 ℃; for 12h; under 760.051 Torr;
DOI:10.1021/acs.joc.7b00485