cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Base Information

Chemical Name:cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol
CAS No.:83196-17-2
Molecular Formula:C₂₃H₂₄N₂O₃
Molecular Weight:376.455
Hs Code.:

cis-2-<benzyl(cyanomethyl)amino>-1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Synonyms:cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Suppliers and Price of cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

There total 8 articles about cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 79076-14-5
{1-[3,4-(methylenedioxy)phenyl]vinyl}lithium

: 83196-16-1
[Benzyl-((R)-2-oxo-cyclopentyl)-amino]-acetonitrile

: 83196-17-2,87014-63-9
{[(1R,2R)-2-(1-Benzo[1,3]dioxol-5-yl-vinyl)-2-hydroxy-cyclopentyl]-benzyl-amino}-acetonitrile

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0040-4039(00)87446-8

Reference yield:

: 6838-66-0
1,2-bis((trimethylsilyl)oxy)cyclopent-1-ene

: 83196-17-2
cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / H₂O / acetone / Ambient temperature

2: 61 percent / benzene / 3 h / Heating

3: 1.) t-BuLi / 1.) pentane, ether, -78 deg C, 1 h, 2.) THF, -78 deg C, 25 min

With water; tert.-butyl lithium; In acetone; benzene;
DOI:10.1021/ja00360a014

Reference yield:

: 3010-05-7
benzylaminoacetonitrile

: 83196-17-2
cis-2--1-<1-(3,4-(methylenedioxy)phenyl)ethenyl>cyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 28 h / Heating

2: 1.) t-BuLi / 1.) pentane, ether, -78 deg C, 1 h, 2.) THF, -78 deg C, 25 min

With tert.-butyl lithium; In methanol;
DOI:10.1021/ja00360a014