2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

Base Information

Chemical Name:2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid
CAS No.:1445800-03-2
Molecular Formula:C₂₀H₁₃ClFN₃O₃S
Molecular Weight:429.859
Hs Code.:

Synonyms:2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

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Chemical Property of 2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

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Technology Process of 2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

There total 4 articles about 2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 1135871-42-9
5-(5-acetylfuran-2-yl)-2-chlorobenzoic acid

: 78364-55-3
1-(6-fluorobenzo[d]thiazol-2-yl)hydrazine

: 1445800-03-2
2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

Guidance literature:: With acetic acid; In ethanol; at 60 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jm400556w

Reference yield:

: 348-40-3
2-amino-6-fluoro-1,3-benzothiazole

: 1445800-03-2
2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate; hydrazine dihydrochloride / 140 °C / Inert atmosphere

2: acetic acid / ethanol / 10 h / 60 °C / Inert atmosphere

With hydrazine dihydrochloride; hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1021/jm400556w

Reference yield:

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: 1445800-03-2
2-chloro-5-(5-(1-(2-(6-fluorobenzothiazol-2-yl)hydrazono)ethyl)furan-2-yl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.08 h / 0 - 5 °C

1.2: 10 h / 20 °C

2.1: acetic acid / ethanol / 10 h / 60 °C / Inert atmosphere

With hydrogenchloride; acetic acid; sodium nitrite; In ethanol; water;
DOI:10.1021/jm400556w