(4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Base Information

Chemical Name:(4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine
CAS No.:1544739-10-7
Molecular Formula:C₂₃H₂₃BrN₂O₂
Molecular Weight:439.352
Hs Code.:
Mol file:1544739-10-7.mol

Synonyms:(4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Suppliers and Price of (4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Chemical Property:

Boiling Point:587.4±50.0 °C(Predicted)
PKA:5.63±0.10(Predicted)
Density:1.322±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

There total 4 articles about (4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1544739-09-4
(4-bromo-5-iodo-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1544739-10-7
(4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Guidance literature:: With potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 18.3333h; Reflux; Inert atmosphere;

Reference yield:

: 84249-14-9
2-amino-4-bromopyridine

: 1544739-10-7
(4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 24 h / 40 °C

3.1: potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18.33 h / Reflux; Inert atmosphere

With potassium fluoride; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; In N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1544739-10-7
(4-bromo-5-vinyl-pyridin-2-yl)-bis-(4-methoxy-benzyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 24 h / 40 °C

3.1: potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18.33 h / Reflux; Inert atmosphere

With potassium fluoride; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; In N,N-dimethyl-formamide; toluene; mineral oil;