6-bromohexanoyl dimethylphenyl silane

Base Information

Chemical Name:6-bromohexanoyl dimethylphenyl silane
CAS No.:147752-76-9
Molecular Formula:C₁₄H₂₁BrOSi
Molecular Weight:313.31
Hs Code.:

Synonyms:6-bromohexanoyl dimethylphenyl silane

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Chemical Property of 6-bromohexanoyl dimethylphenyl silane

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Technology Process of 6-bromohexanoyl dimethylphenyl silane

There total 1 articles about 6-bromohexanoyl dimethylphenyl silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 174710-92-0
[1,3]Dithian-2-yl-dimethyl-phenyl-silane

: 147752-76-9
6-bromohexanoyl dimethylphenyl silane

Guidance literature:: With n-butyllithium; Celite; boron trifluoride diethyl etherate; mercury(II) oxide; Yield given. Multistep reaction; 1.) THF, hexane, 0 deg C, 30 min; -30 deg C, 1.5 h, 2.) THF, H₂O, room temperature, 1 h;
DOI:10.1021/jo9711302

Reference yield: 79.0%

: 147752-76-9
6-bromohexanoyl dimethylphenyl silane

: 65335-82-2
[dimethyl(phenyl)silyloxy]cyclohexane

: 91356-96-6
1-(Dimethyl-phenyl-silanyl)-hexan-1-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 6h; Yields of byproduct given;
DOI:10.1016/S0040-4039(00)91780-5

Reference yield: 40.0%

: 33797-51-2
eschenmoser's salt

: 147752-76-9
6-bromohexanoyl dimethylphenyl silane

: 2-(4-bromobutyl)-1-(dimethylphenyl)silylprop-2-en-1-one

: 2-(4-iodobutyl)-1-(dimethylphenyl)silylprop-2-en-1-one

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; Title compound not separated from byproducts; 1.) -78 deg C, 1 h; 2.) room temp., 1.5 h;
DOI:10.1055/s-1995-3907