methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

Base Information

Chemical Name:methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate
CAS No.:106344-76-7
Molecular Formula:C₂₀H₂₉NO₃SSi
Molecular Weight:391.607
Hs Code.:

Synonyms:methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

Suppliers and Price of methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

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Technology Process of methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

There total 2 articles about methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 81355-65-9
methyl 1-tert-butyldimethylsilyl-4-oxo-2-azetidine-α-butynoate

: 108-98-5
thiophenol

: 106344-76-7
methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

: 106344-75-6
methyl(Z)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

Guidance literature:: With triethylamine; In methanol; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.34.1434

Reference yield:

: 81355-49-9
C₁₂H₂₀LiNOSi

: 106344-76-7
methyl(E)-1-tert-butyldimethylsilyl-4-oxo-β-phenylthio-2-azetidine-α-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / tetrahydrofuran / 1.33 h / -78 °C

2: 7 percent / triethylamine / methanol / 0.5 h / Ambient temperature

With triethylamine; In tetrahydrofuran; methanol;
DOI:10.1248/cpb.34.1434