2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

Base Information

Chemical Name:2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine
CAS No.:1131450-96-8
Molecular Formula:C₁₈H₂₁NO₄
Molecular Weight:323.306
Hs Code.:

Synonyms:2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

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Chemical Property of 2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

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Technology Process of 2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

There total 5 articles about 2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1131450-95-7
(Z)-2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)-benzylidene)ethanamine

: 1131450-96-8
2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

Guidance literature:: With sodium tetrahydroborate; In methanol; for 2h; Heating / reflux;

Reference yield:

: 710336-81-5
dideuterocatechol

: 1131450-96-8
2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

Guidance literature:: Multi-step reaction with 5 steps

1: water-d2; potassium carbonate / 1-methyl-pyrrolidin-2-one / 2.5 h / 110 °C

2: ammonium acetate / acetic acid / 4 h / Heating / reflux

3: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / Heating / reflux

4: dichloromethane / 16 h / 20 °C / Molecular sieve

5: sodium tetrahydroborate / methanol / 2 h / Heating / reflux

With sodium tetrahydroborate; lithium aluminium tetrahydride; ammonium acetate; water-d2; potassium carbonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; diethyl ether; dichloromethane; acetic acid;

Reference yield:

: 1131450-92-4
2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)ethanamine

: 1131450-96-8
2-(2,2-d2-benzo[d][1,3]dioxol-5-yl)-N-(2,3-(dimethoxy-d6)benzyl)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 16 h / 20 °C / Molecular sieve

2: sodium tetrahydroborate / methanol / 2 h / Heating / reflux

With sodium tetrahydroborate; In methanol; dichloromethane;