(2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

Base Information

Chemical Name:(2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide
CAS No.:1349043-31-7
Molecular Formula:C₁₉H₁₈Cl₃N₃O₂
Molecular Weight:426.73
Hs Code.:

Synonyms:(2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

Suppliers and Price of (2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

Chemical Property:

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Technology Process of (2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

There total 9 articles about (2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-79-4,22031-64-7
cinnamamide

: 1349043-31-7
(2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

Guidance literature:: Multi-step reaction with 6 steps

1: toluene / 4 h / Reflux

2: thionyl chloride / toluene / 2 h / Reflux

3: acetone / 2 h / Reflux

4: ammonium hydroxide / tetrahydrofuran / Cooling

5: 1,4-dioxane / 12 h / Reflux

6: 1,4-dioxane / 2 h / Reflux

With ammonium hydroxide; thionyl chloride; In tetrahydrofuran; 1,4-dioxane; acetone; toluene;
DOI:10.2174/092986712804485971

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 1349043-31-7
(2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride / tetrahydrofuran / 2 h / Reflux

2: ammonium hydroxide / water / Cooling

3: toluene / 4 h / Reflux

4: thionyl chloride / toluene / 2 h / Reflux

5: acetone / 2 h / Reflux

6: ammonium hydroxide / tetrahydrofuran / Cooling

7: 1,4-dioxane / 12 h / Reflux

8: 1,4-dioxane / 2 h / Reflux

With ammonium hydroxide; thionyl chloride; In tetrahydrofuran; 1,4-dioxane; water; acetone; toluene;
DOI:10.2174/092986712804485971

Reference yield:

: 16535-67-4
(2E)-3-phenyl-N-[1-hydroxy-2,2,2-trichloroethyl]-2-acrylamide

: 1349043-31-7
(2E)-3-phenyl-N-[1-(4-tolylamino)oxoformylamino-2,2,2-trichloroethyl]-2-acrylamide

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / toluene / 2 h / Reflux

2: acetone / 2 h / Reflux

3: ammonium hydroxide / tetrahydrofuran / Cooling

4: 1,4-dioxane / 12 h / Reflux

5: 1,4-dioxane / 2 h / Reflux

With ammonium hydroxide; thionyl chloride; In tetrahydrofuran; 1,4-dioxane; acetone; toluene;
DOI:10.2174/092986712804485971