5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine

Base Information

Chemical Name:5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine
CAS No.:153625-46-8
Molecular Formula:C₁₈H₁₃N₅O₅S
Molecular Weight:411.398
Hs Code.:

Synonyms:5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine

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Technology Process of 5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine

There total 2 articles about 5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 153625-38-8
5-amino-6-cyano-1-ethoxycarbonyl-8-mercapto-4-oxo-3-phenylphthalazine

: 153625-46-8
5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine

Guidance literature:: With sulfuric acid; nitric acid; In water; for 0.166667h; Heating;

Reference yield:

: 123542-47-2
ethyl 5-amino-3,4-dihydro-4-oxo-3-phenylthieno<3,4-d>pyridazine-1-carboxylate

: 153625-46-8
5-amino-6-cyano-1-ethoxycarbonyl-4-oxo-8-mercapto-7-nitro-3-phenylphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 5 h / Heating

2: 78 percent / concd H₂SO₄, fuming HNO₃ / H₂O / 0.17 h / Heating

With pyridine; sulfuric acid; nitric acid; In water;