Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

Base Information

Chemical Name:Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate
CAS No.:1177428-61-3
Molecular Formula:C₁₈H₁₇NOSe
Molecular Weight:342.299
Hs Code.:

Synonyms:Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

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Chemical Property of Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

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Technology Process of Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

There total 3 articles about Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1666-13-3
diphenyl diselenide

: N-phenethyl-N-prop-2-ynylcarbamoyl chloride

: 1177428-61-3
Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

Guidance literature:: diphenyl diselenide; With methanol; sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

N-phenethyl-N-prop-2-ynylcarbamoyl chloride; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/hc.21217

Reference yield:

: 58185-47-0
N-phenethyl-N-prop-2-ynylamine

: 1177428-61-3
Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

2.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

With pyridine; methanol; sodium tetrahydroborate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hc.21217

Reference yield:

: 64-04-0
phenethylamine

: 1177428-61-3
Se-phenyl N-(2-phenylethyl)-N-(prop-2-ynyl)carbamoselenoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: neat (no solvent) / 20 °C / Cooling with ice; Inert atmosphere

2.1: pyridine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

With pyridine; methanol; sodium tetrahydroborate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hc.21217