N-triphenylphosphinimid

Base Information

Chemical Name:N-triphenylphosphinimid
CAS No.:33354-65-3
Molecular Formula:C₃₂H₂₉N₄P
Molecular Weight:500.583
Hs Code.:

N-<p-(Dimethylaminophenylazo)phenyl>triphenylphosphinimid

Synonyms:N-triphenylphosphinimid

Suppliers and Price of N-triphenylphosphinimid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-triphenylphosphinimid

Chemical Property:

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Technology Process of N-triphenylphosphinimid

There total 3 articles about N-triphenylphosphinimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: C₁₄H₁₆N₆

: 603-35-0
triphenylphosphine

: 33354-65-3
N-triphenylphosphinimid

Guidance literature:: In toluene; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2017.04.039

Reference yield:

: 539-17-3
N,N-dimethyl-4,4'-azodianiline

: 33354-65-3
N-triphenylphosphinimid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 °C

1.2: 0 °C

2.1: toluene / 2.5 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; sodium nitrite; In water; toluene; 2.1: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2017.04.039