Technology Process of C24H30O3S
There total 6 articles about C24H30O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tet.2011.03.114
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol / 20 °C
2.1: sodium periodate / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C
3.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / 0 - 20 °C
3.2: 0 °C
4.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; water; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.03.114
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium periodate / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C
2.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / 0 - 20 °C
2.2: 0 °C
3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.03.114
