4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

Base Information

Chemical Name:4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)
CAS No.:228550-69-4
Molecular Formula:C₅₉H₆₆O₁₀S₂
Molecular Weight:999.299
Hs Code.:

Synonyms:4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

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Chemical Property of 4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

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Technology Process of 4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

There total 1 articles about 4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 211934-98-4
2,6-anhydro-4,5,7-tri-O-benzyl-1-(propane-1,3-diyl-dithioacetal)-1,3-dideoxy-D-lyxo-hept-1-enitol

: 228550-69-4
4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - -5 ℃; for 2h;

Reference yield:

: 228550-69-4
4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

: (2R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-2-carboxylic acid

Guidance literature:: With N-Bromosuccinimide; water; In tetrahydrofuran; for 0.5h;

Reference yield:

: 228550-69-4
4,5,7-tri-O-benzyl-3-deoxy-1-(propane-1,3-diyl dithioacetal)-α-D-lyxo-heptopyranosyl-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

: [methyl (4,5,7-tri-O-benzyl-3-deoxy-α-D-lyxo-hept-2-ulopyranosid)onate]-(2->6)-(methyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside)

Guidance literature:: Multi-step reaction with 2 steps

1: NBS; H₂O / tetrahydrofuran / 0.5 h

2: methanol; diethyl ether

With N-Bromosuccinimide; water; In tetrahydrofuran; methanol; diethyl ether; 1: oxidative hydrolysis / 2: Esterification;