Technology Process of C62H66NO18P
There total 5 articles about C62H66NO18P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: H2 / Pd-C
2: benzoyl peroxide
3: HCl / acetonitrile
4: N-iodosuccinimide, 4 Angstroem sieves / CH2Cl2; tetrahydrofuran
5: H2 / Pd-C / ethyl acetate / 2.5 h / 3102.9 Torr / Ambient temperature
6: bovine intestinal alkaline phosphatase
7: benzoyl peroxide / acetonitrile / 2 h / 0 °C
8: N-iodosuccinimide, 4 Angstroem sieves / CH2Cl2; tetrahydrofuran
With
hydrogenchloride; N-iodo-succinimide; 4 A molecular sieve; hydrogen; dibenzoyl peroxide;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/0960-894X(96)00321-6
- Guidance literature:
-
Multi-step reaction with 6 steps
1: HCl / acetonitrile
2: N-iodosuccinimide, 4 Angstroem sieves / CH2Cl2; tetrahydrofuran
3: H2 / Pd-C / ethyl acetate / 2.5 h / 3102.9 Torr / Ambient temperature
4: bovine intestinal alkaline phosphatase
5: benzoyl peroxide / acetonitrile / 2 h / 0 °C
6: N-iodosuccinimide, 4 Angstroem sieves / CH2Cl2; tetrahydrofuran
With
hydrogenchloride; N-iodo-succinimide; 4 A molecular sieve; hydrogen; dibenzoyl peroxide;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/0960-894X(96)00321-6
- Guidance literature:
-
Multi-step reaction with 4 steps
1: H2 / Pd-C / ethyl acetate / 2.5 h / 3102.9 Torr / Ambient temperature
2: bovine intestinal alkaline phosphatase
3: benzoyl peroxide / acetonitrile / 2 h / 0 °C
4: N-iodosuccinimide, 4 Angstroem sieves / CH2Cl2; tetrahydrofuran
With
N-iodo-succinimide; 4 A molecular sieve; hydrogen; dibenzoyl peroxide;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/0960-894X(96)00321-6