3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

Base Information

Chemical Name:3,4-di(4-octyloxyphenyl)-1-tosylpyrrole
CAS No.:1357168-94-5
Molecular Formula:C₃₉H₅₁NO₄S
Molecular Weight:629.904
Hs Code.:

Synonyms:3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

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Technology Process of 3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

There total 2 articles about 3,4-di(4-octyloxyphenyl)-1-tosylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 849939-22-6
3,4-dibromo-1-(4-methylbenzenesulfonyl)-1H-pyrrole

: 1206159-45-6
2-(4-octyloxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1357168-94-5
3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; at 20 ℃; for 24h; Inert atmosphere; Reflux;
DOI:10.1039/c2cc17282h

Reference yield:

: 96693-05-9
1-bromo-4-octyloxybenzene

: 1357168-94-5
3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / 24 h / 100 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane / 24 h / 20 °C / Inert atmosphere; Reflux

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; In 1,2-dimethoxyethane;
DOI:10.1039/c2cc17282h

Reference yield:

: 1357168-94-5
3,4-di(4-octyloxyphenyl)-1-tosylpyrrole

: 1357168-96-7
3,4-di(4-octyloxyphenyl)pyrrole

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c2cc17282h