C₂₂H₂₂O₅

Base Information

Chemical Name:C₂₂H₂₂O₅
CAS No.:1419777-81-3
Molecular Formula:C₂₂H₂₂O₅
Molecular Weight:366.414
Hs Code.:

C<sub>22</sub>H<sub>22</sub>O<sub>5</sub>

Synonyms:C₂₂H₂₂O₅

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Chemical Property of C₂₂H₂₂O₅

Chemical Property:

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Technology Process of C₂₂H₂₂O₅

There total 11 articles about C₂₂H₂₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1419777-75-5
C₂₂H₂₄O₅

: 1419777-81-3
C₂₂H₂₂O₅

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 3h;
DOI:10.1021/ol303482k

Reference yield:

: 480-34-2
eugenin

: 1419777-81-3
C₂₂H₂₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone / 24 h / Reflux

2.1: 2 h / 200 °C

3.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone / 24 h / Reflux

4.1: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) / tetrahydrofuran / 3 h / Reflux

5.1: 2,6-dimethylpyridine; osmium(VIII) oxide; sodium periodate / 1,4-dioxane; water; tert-butyl alcohol / 0.5 h

6.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.08 h / 0 °C

7.1: phosphorus tribromide / tetrahydrofuran; dichloromethane / 4.5 h / 0 °C

8.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

8.2: 0.5 h / -78 °C

9.1: methanol; lithium borohydride / tetrahydrofuran; diethyl ether / 5 h

10.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C

With 2,6-dimethylpyridine; methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; lithium borohydride; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); sodium hexamethyldisilazane; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; dimethyl sulfoxide; acetone; tert-butyl alcohol;
DOI:10.1021/ol303482k

Reference yield:

: 1013-69-0
eugenin

: 1419777-81-3
C₂₂H₂₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium carbonate / acetone / 12 h / 20 °C

2.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone / 24 h / Reflux

3.1: 2 h / 200 °C

4.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone / 24 h / Reflux

5.1: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) / tetrahydrofuran / 3 h / Reflux

6.1: 2,6-dimethylpyridine; osmium(VIII) oxide; sodium periodate / 1,4-dioxane; water; tert-butyl alcohol / 0.5 h

7.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.08 h / 0 °C

8.1: phosphorus tribromide / tetrahydrofuran; dichloromethane / 4.5 h / 0 °C

9.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

9.2: 0.5 h / -78 °C

10.1: methanol; lithium borohydride / tetrahydrofuran; diethyl ether / 5 h

11.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C

With 2,6-dimethylpyridine; methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; lithium borohydride; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); sodium hexamethyldisilazane; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; dimethyl sulfoxide; acetone; tert-butyl alcohol;
DOI:10.1021/ol303482k