3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester

Base Information

Chemical Name:3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester
CAS No.:87119-52-6
Molecular Formula:C₃₈H₄₂O₇S
Molecular Weight:642.813
Hs Code.:

Synonyms:3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester

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Technology Process of 3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester

There total 2 articles about 3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2935-90-2
Methyl 3-mercaptopropionate

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 87119-52-6
3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester

Guidance literature:: With Molekularsieb 4 A; boron trifluoride diethyl etherate; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 87119-52-6
3-<(2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl)thio>propionsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaH / CH₂Cl₂ / 2.5 h / Ambient temperature

2: 95 percent / 0.1 M BF₃*OEt₂, Molekularsieb 4 A / CH₂Cl₂ / 2 h / Ambient temperature

With Molekularsieb 4 A; boron trifluoride diethyl etherate; sodium hydride; In dichloromethane;