1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde

Base Information

• Chemical Name: 1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde
• CAS No.: 151409-85-7
• Molecular Formula: C₁₅H₁₈N₂O₂
• Molecular Weight: 258.32
• DSSTox Substance ID: DTXSID401214224

Synonyms:1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde;151409-85-7;1-(2-Morpholinoethyl)-1H-indole-3-carbaldehyde;1-(2-morpholin-4-ylethyl)indole-3-carbaldehyde;DTXSID401214224;AKOS000301694;1-[2-(4-Morpholinyl)ethyl]-1H-indole-3-carboxaldehyde;1-[2-(morpholin-4-yl)ethyl]-1H-indole-3-carbaldehyde

Chemical Property of 1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde

Chemical Property:

• XLogP3: 1.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 258.136827821
• Heavy Atom Count: 19
• Complexity: 305

Purity/Quality:

98%min ^*data from raw suppliers

1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1COCCN1CCN2C=C(C3=CC=CC=C32)C=O

Technology Process of 1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde

There total 1 articles about 1-(2-Morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.4%

Indole-3-carboxaldehyde (487-89-8,1228547-52-1) + 4-(2-chloroethyl)morpholine hydrochride (3647-69-6) → 1-(2-morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde (151409-85-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 48h;

DOI:10.1039/d0nj01477j

Reference yield: 35.0%

4,4-difluoro-1,3,5,7-tetramethyl-8-(4-hydroxyphenyl)-4-bora-3a,4a-diaza-s-indacene + 1-(2-morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde (151409-85-7) → Lyso-Red

Guidance literature:

With piperidine; acetic acid; In 2-methoxy-ethanol; at 80 - 110 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.dyepig.2018.03.015

Reference yield: 35.0%

4,4-difluoro-1,3,5,7-tetramethyl-8-(4-hydroxyphenyl)-4-bora-3a,4a-diaza-s-indacene + 1-(2-morpholin-4-yl-ethyl)-1H-indole-3-carbaldehyde (151409-85-7) → Lyso-NIR

Guidance literature:

With piperidine; acetic acid; In 2-methoxy-ethanol; at 80 - 140 ℃; for 10h; Inert atmosphere;

DOI:10.1039/c7tb00489c

upstream raw materials:

Indole-3-carboxaldehyde

4-(2-chloroethyl)morpholine hydrochride

Downstream raw materials:

[1-(2-morpholin-4-yl-ethyl)-1H-indol-3-ylmethyl]-p-tolyl-amine

(4-chloro-phenyl)-[1-(2-morpholin-4-yl-ethyl)-1H-indol-3-ylmethyl]-amine

(4-methoxy-phenyl)-[1-(2-morpholin-4-yl-ethyl)-1H-indol-3-ylmethyl]-amine

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