Technology Process of C22H29F3O6S
There total 6 articles about C22H29F3O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C21H30BrNO3;
With
methanesulfonic acid; zinc;
In
tetrahydrofuran;
Inert atmosphere;
Reflux;
With
hydrogenchloride;
In
tetrahydrofuran; water;
Heating;
trifluoromethylsulfonic anhydride;
In
dichloromethane;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/chem.201300827
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / Inert atmosphere
3.1: titanium(IV) isopropylate; C23H16N2O2 / dichloromethane / -40 °C / Inert atmosphere
3.2: 48 h / -40 °C / Inert atmosphere
4.1: dichloromethane / 2.5 h / 0 °C / Inert atmosphere
5.1: methanesulfonic acid; zinc / tetrahydrofuran / Inert atmosphere; Reflux
5.2: Heating
5.3: 2 h / 0 °C / Inert atmosphere
With
titanium(IV) isopropylate; methanesulfonic acid; C23H16N2O2; silica gel; sodium hydride; pyridinium chlorochromate; zinc;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201300827
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dichloromethane / 2.5 h / 0 °C / Inert atmosphere
2.1: methanesulfonic acid; zinc / tetrahydrofuran / Inert atmosphere; Reflux
2.2: Heating
2.3: 2 h / 0 °C / Inert atmosphere
With
methanesulfonic acid; zinc;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201300827
