methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

Base Information

Chemical Name:methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate
CAS No.:154371-60-5
Molecular Formula:C₂₅H₂₃F₅N₆O₂
Molecular Weight:534.489
Hs Code.:

Synonyms:methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

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Chemical Property of methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

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Technology Process of methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

There total 3 articles about methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 154371-59-2
methyl 2-butyl-4-pentafluoroethyl-1-<4-(2-cyanophenyl)phenyl>methylimidazole-5-carboxylate

: 154371-60-5
methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

Guidance literature:: With trimethylsilylazide; di(n-butyl)tin oxide; In toluene; for 18h; Heating;
DOI:10.1080/00397919308011184

Reference yield:

: 1027367-55-0
4'-(2-Butyl-5-formyl-4-pentafluoroethyl-imidazol-1-ylmethyl)-biphenyl-2-carbonitrile

: 154371-60-5
methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: NaClO₂, KH₂PO₄, 2-methylbut-2-ene / 2-methyl-propan-2-ol; H₂O

2: diethyl ether

3: 64 percent / Bu₂SnO, Me₃SiN₃ / toluene / 18 h / Heating

With sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene; trimethylsilylazide; di(n-butyl)tin oxide; In diethyl ether; water; toluene; tert-butyl alcohol;
DOI:10.1080/00397919308011184

Reference yield:

: 1027576-16-4
2-Butyl-3-(2'-cyano-biphenyl-4-ylmethyl)-5-pentafluoroethyl-3H-imidazole-4-carboxylic acid

: 154371-60-5
methyl 2-butyl-4-pentafluoroethyl-1-<4-<2-(5-tetrazolo)phenyl>phenyl>methylimidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 64 percent / Bu₂SnO, Me₃SiN₃ / toluene / 18 h / Heating

With trimethylsilylazide; di(n-butyl)tin oxide; In diethyl ether; toluene;
DOI:10.1080/00397919308011184