N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

Base Information

Chemical Name:N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid
CAS No.:344462-93-7
Molecular Formula:C₁₄H₂₂BNO₆S
Molecular Weight:343.209
Hs Code.:

Synonyms:N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

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Chemical Property of N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

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Technology Process of N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

There total 5 articles about N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.2%

: 353235-95-7
N-(t-butoxycarbonyl)-N-(methylsulfonyl)-N-(2-(4-(4,4,5,5-tetramethyl(1,3,2-dioxaborolan-2-yl))phenyl)ethyl)amine

: 344462-93-7
N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

Guidance literature:: With sodium periodate; ammonium acetate; In water; acetone;

Reference yield:

: 353235-93-5
N-(2-(4-iodophenyl)ethyl)-N-(methylsulfonyl)amine

: 344462-93-7
N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / dichloromethane / 20 °C

2: triethylamine / 1,1'-bis(diphenylphosphino) ferrocene-dichloropalladium (II)-CH₂Cl₂ complex / acetonitrile / 8 h / 70 - 74 °C

3: sodium periodate; ammonium acetate / acetone / 20 °C

With dmap; sodium periodate; ammonium acetate; triethylamine; 1,1'-bis(diphenylphosphino) ferrocene-dichloropalladium (II)-CH₂Cl₂ complex; In dichloromethane; acetone; acetonitrile;

Reference yield:

: 64-04-0
phenethylamine

: 344462-93-7
N-carbamic acid tert-butyl ester-N-methanesulfonamide-N-phenethyl-4-boronic acid

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 1.67 h / 10 - 20 °C

2: sulfuric acid; iodine; acetic acid; periodic acid / water / 3 h / 20 - 75 °C

3: dmap / dichloromethane / 20 °C

4: triethylamine / 1,1'-bis(diphenylphosphino) ferrocene-dichloropalladium (II)-CH₂Cl₂ complex / acetonitrile / 8 h / 70 - 74 °C

5: sodium periodate; ammonium acetate / acetone / 20 °C

With dmap; sodium periodate; sulfuric acid; ammonium acetate; iodine; acetic acid; periodic acid; triethylamine; 1,1'-bis(diphenylphosphino) ferrocene-dichloropalladium (II)-CH₂Cl₂ complex; In dichloromethane; water; acetone; acetonitrile;