1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Base Information

Chemical Name:1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline
CAS No.:82168-92-1
Molecular Formula:C₂₀H₁₇N₃O₂
Molecular Weight:331.374
Hs Code.:

Synonyms:1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Suppliers and Price of 1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

There total 7 articles about 1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 82157-87-7
5-(2-aminophenyl)-3-ethoxycarbonyl-2-methyl-1-phenyl-1H-pyrrole

: 82168-92-1
1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Guidance literature:: With acetic acid; sodium nitrite; In water; at 0 - 5 ℃; for 1h;

Reference yield:

: 82157-83-3
4-Ethoxycarbonyl-5-methyl-2-(2-nitrophenyl)-1-phenylpyrrole

: 82168-92-1
1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / H₂ / 10percent palladium on charcoal

2: 85 percent / acetic acid, sodium nitrite / H₂O / 1 h / 0 - 5 °C

With hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In water;

Reference yield:

: 111277-26-0
4-Bromo-2-methyl-5-(2-nitro-phenyl)-1-phenyl-1H-pyrrole-3-carboxylic acid ethyl ester

: 82168-92-1
1-Ethoxycarbonyl-2-methyl-3-phenylpyrrolo<3,2-c>cinnoline

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / aq. TiCl₃ / acetic acid / Ambient temperature; overnight

2: 1) aq. HCl, NaNO₂ 2) 50 percent aq. hypophosphorous acid / 1) 0 to 5 deg C, 30 min. 2) room temperature, overnight

With hydrogenchloride; titanium(III) chloride; hypophosphorous acid; sodium nitrite; In acetic acid;
DOI:10.1002/jhet.5570230522