Technology Process of C39H47N7O9
There total 7 articles about C39H47N7O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 1.5h;
Cooling with ice;
DOI:10.1021/ja400970n
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16.5 h / 20 °C / Cooling with ice
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C
3.1: acetic acid / water / 16 h / 20 °C
3.2: 2 h / 20 °C
4.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 16 h / 20 °C
5.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice
6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C / Cooling with ice
7.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice
With
potassium hydrogencarbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja400970n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 16 h / 20 °C
2: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C / Cooling with ice
4: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice
With
potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja400970n
