Technology Process of C20H18FN3O5
There total 8 articles about C20H18FN3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
chloroform;
at 25 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: nitric acid; acetic anhydride; acetic acid / chloroform; water / 0.5 h / 0 °C
2.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 24 h / 125 °C
2.2: 0.25 h / 20 °C
3.1: potassium peroxymonosulfate / N,N-dimethyl-formamide / 18 h / 20 °C
4.1: thionyl chloride; N,N-dimethyl-formamide / chloroform / 0.5 - 18 h / 20 °C / Heating / reflux
5.1: triethylamine / chloroform / 18 h / 25 °C
With
potassium peroxymonosulfate; thionyl chloride; nitric acid; acetic anhydride; acetic acid; N,N-dimethyl-formamide dimethyl acetal; triethylamine; N,N-dimethyl-formamide;
In
chloroform; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium peroxymonosulfate / N,N-dimethyl-formamide / 18 h / 20 °C
2: thionyl chloride; N,N-dimethyl-formamide / chloroform / 0.5 - 18 h / 20 °C / Heating / reflux
3: triethylamine / chloroform / 18 h / 25 °C
With
potassium peroxymonosulfate; thionyl chloride; triethylamine; N,N-dimethyl-formamide;
In
chloroform; N,N-dimethyl-formamide;