2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

Base Information

Chemical Name:2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate
CAS No.:1230076-22-8
Molecular Formula:C₂₅H₃₀O₉
Molecular Weight:474.508
Hs Code.:

Synonyms:2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

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Chemical Property of 2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

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Technology Process of 2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

There total 1 articles about 2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 28915-80-2,40591-53-5,40591-54-6,40591-55-7,120449-19-6,120449-20-9,143332-42-7,148081-39-4,151413-57-9,151413-58-0
2,3,4-tri-O-acetyl-L-rhamnopyranose

: 120870-47-5
2-(1-hexyn-1-yl)benzoic acid

: 1230076-22-8
2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

Guidance literature:: 2-(1-hexyn-1-yl)benzoic acid; With thionyl chloride; Heating;

2,3,4-tri-O-acetyl-L-rhamnopyranose; With dmap; triethylamine; In dichloromethane; at 20 ℃; Further stages.;
DOI:10.1016/j.tetlet.2008.04.017

Reference yield: 99.0%

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 1230076-22-8
2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

: methyl 2,3,4-tri-O-acetyl-α-L-rhamnosyl-(1→6)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 3h; Molecular sieve;
DOI:10.1002/anie.201103409

Reference yield: 93.0%

: 1230076-22-8
2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate

: N⁴-benzoylcytosine

: C₂₅H₂₉N₃O₁₁

Guidance literature:: 2,3,4-tri-O-acetyl-L-rhamnopyranosyl ortho-hexynylbenzoate; N⁴-benzoylcytosine; With N,O-Bis(trimethylsilyl)trifluoroacetamide; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; acetonitrile; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.joc.1c00151