8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside

Base Information Edit

Chemical Name:8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside
CAS No.:108167-19-7
Molecular Formula:C₃₄H₄₆O₁₀
Molecular Weight:614.733
Hs Code.:
Mol file:108167-19-7.mol

Synonyms:8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside

Suppliers and Price of 8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside

There total 3 articles about 8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 34957-73-8
methyl 9-hydroxynonanoate

: 86861-46-3
3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranosyl bromide

: 108167-19-7
8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1021/jo00389a039

Reference yield:

: 80738-50-7
1,3,6-tri-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranose

: 108167-19-7
8-(methoxycarbonyl)octyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: HBr / CH₂Cl₂ / 2 h / 0 °C

2: 73 percent / sym-collidine, silver trifluoromethanesulfonate, 4-A molecular sieves / CH₂Cl₂ / 15 h / Ambient temperature

With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; hydrogen bromide; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/jo00389a039